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紫草乙醇浸膏精制方法的研究
http://www.100md.com 《中华医药杂志》 2005年第10期
乙醇浸膏,,紫草;乙醇浸膏;精制,1仪器与试药,2方法与结果,3结论与讨论,【参考文献】
     【摘要】 目的 研究紫草乙醇浸膏的精制方法。方法 碱溶酸沉法,大孔树脂吸附法,超临界CO2萃取法,含水乙醇-石油醚萃取法,铜盐络合法。结果 以外观性状、收率和萘醌总色素的含量为指标,对5种方法所得精制产品进行了比较。结论 含水乙醇-石油醚萃取法较适于工厂生产中紫草乙醇浸膏的精制。

    【关键词】 紫草;乙醇浸膏;精制

    Study on purification methods for the ethanol-extracts of radix arnebiae

    YANG Wen-yu,CHEN Bin.

    Faculty of Bioengineering, Xihua University, Chengdu Sichuan 610039,China

    【Abstract】 Objective To develop methods for purifying the ethanol-extracts of Radix Arnebiae.Methods (I) pH control, (II) absorption by macro-porous resin, (III) super critical carbon dioxide extraction, (IV) liquid-liquid extraction between ethanol (contained water) and petroleum ether, (V) creation of Cu2+ complex.Results Samples from five methods were evaluated though physic status, yield and the content of total hydroxyl naphthoquinones.Conclusion Method IV is an effective process to purify the ethanol-extracts of gromwell in scale.

    【Key words】 gromwell (Radix Arnebiae);ethanol extract;purification

    中药紫草具有凉血活血、解毒透疹的功效 ......

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