山茱萸_____山茱萸；总皂苷；提取；含量测定

山茱萸总皂苷的提取分离与含量测定

http://www.100md.com 《第四军医大学学报》 2003年第5期

山茱萸,,山茱萸；总皂苷；提取；含量测定,0引言,1材料和方法,2结果,3讨论,【参考文献】

     Extraction and determination of total saponins from Cornus officinalis Sieb. et Zucc.

    WU Hong, LIANG Heng, LIU YongHong, YUAN ZhongHai

    Separation science institute, School of Life Sciences and Technology, Xian Jiaotong University, Xian 710049, China, Department of Chemistry, Faculty of Preclinical Medicine, Fourth Military Medical University, Xian 710033, China

    【Abstract】 AIM: To review effects of different methods of extracting total saponins from Cornus officinalis so as to provide an effective way to accurately determine total saponins. METHODS: ① Methanol reflux, ② Ether degreasing Methanol reflux, ③ Ultrasonic abstraction, ④ Method of macroreticular absorption resin and ⑤ Ethanol reflux were compared. With Ginsenoside Re and Oleanolic acid as standard, chromatometry was used respectively to determine total saponins of different extraction solution. RESULTS: The content of total saponins determined by methods of ①, ②, ③ and ⑤ was 5.95%, 6.98%; 2.87%, 3.12%; 3.80%, 3.92%; 6.17% and 8.13% respectively, and by method of ④, it was 1.52% and 1.73%. CONCLUSION: Different extracting methods have much influence on determining total saponins in Cornus officinalis. ......

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