三鼎_____三鼎丹胶囊；士的宁；薄层扫描

三鼎丹胶囊中士的宁的含量测定

http://www.100md.com 《时珍国医国药》 2006年第1期

三鼎,,三鼎丹胶囊；士的宁；薄层扫描,1实验条件,2方法与结果,3讨论,参考文献：

     摘要：目的建立测定三鼎丹胶囊中士的宁的含量测定方法。方法以甲苯丙酮乙醇浓氨溶液(16∶12∶1∶4)的上层溶液为展开剂，采用双波长反射锯齿扫描法，测定波长λS=254 nm，参比波长λR=325 nm，测定士的宁的含量。结果样品平均回收率为99.5%，板内RSD=4.48%(n=5)。结论此测定方法简单可行，重现性好，可作为该药质量控制的参考依据。

    关键词：三鼎丹胶囊；士的宁；薄层扫描

    Quantitative Determination of Strychnine in SanDingDan Capsule by TLCScanning

    JI Shengguo, WANG Dong, LI E, HE Fang, SONG Sa

    (1.College of Pharmacy, Zhengzhou University, Zhengzhou 450052, China; 2.Henan College of Traditional Chinese Medicine, Zhengzhou, Henan 450008,China; 3. Traditional Chinese Medicine Hospital of Jiaozuo, Henan 454100, China)

    Abstract：ObjectiveTo determine the content of Strychnine in SanDingDan Capsule. MethodsTLC was used with detecting wavelength 254 nm and reference wavelength 325 nm. ResultsThe average recovery was 99.15% ......

百拇医药网 http://www.100md.com/html/DirDu/2006/04/25/96/87/76.htm

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