荆芥防风药对的HPLC特征图谱研究(3)
[3] 徐国龙,陈维华,张明淮,等.药对与临床[M].合肥:安徽科学出版社,2003:32.
[4] 黄晓青,朱凯云.消风散的药理药效研究及临床应用概况[J].江苏中医药,2012,43(1):69.
[5] 华峰.驱风一字散加味联合穿心莲滴眼液治疗春季结膜炎临床观察[J].基层园地,1998,8(1):56.
[6] 焦灵利.荆防抗感泡腾片的研制与药效学研究[D].南京:南京中医药大学,2007.
[7] 曾南,沈映君,刘旭光,等.荆芥挥发油抗炎作用研究[J].中药药理与临床,1998,14(6)∶24.
[8] 李淑荣,唐光菊.荆芥与防风的药理作用研究[J].中药材,1989,12(6):37.
[9] 葛卫红. 荆芥、防风挥发油抗炎作用的实验研究[J].成都中医药大学学报,2003,25(1):55.
[10] 朱慧,张良,喻斌,等. 荆芥内酯的一般药理学研究[J]. 中国实验方剂学杂志,2011,17(6):237.
[11] 钱雯,单鸣秋,丁安伟.荆芥饮片HPLC指纹图谱研究[J].中成药,2011,33(5):733.
[12] 胥庆华,刘丽云,赵瑞华.中药药对大全[M]. 北京:中国中药出版社,1996:360.
HPLC specific chromatograms of drug pair of Schizonepetae
Herba and Saposhnikoviae Radix
YU Li-xia,SHAN Ming-qiu,DING An-wei*
(Jiangsu Key Laboratory for Traditional Chinese Medicine Formulae Research,Nanjing University of
Chinese Medicine,Nanjing 210023,China)
[Abstract] In this experiment,the HPLC specific chromatogram was adopted,with Agilent Extend-C18 (4.6 mm×250 mm,5 μm) as the chromatographic column,and 0.5‰ trifluoroacetic acid and acetonitrile as the mobile phase for gradient elution,so as to establish specific chromatograms for drug pair of Schizonepetae Herba and Saposhnikoviae Radix from different producing area,identify 12 common characteristic peaks,and obtain the comparison specific chromatography of drug pair of Schizonepetae Herba and Saposhnikoviae Radix. The method is simple,accurate and highly reproducible,and thus can be used as the basis for the quality control of the drug pair.
[Key words] Schizonepeta Herba;Saposhnikovia Radix;drug pair;specific chromatogram
doi:10.4268/cjcmm20140425, 百拇医药(于丽霞 单鸣秋 丁安伟)
[4] 黄晓青,朱凯云.消风散的药理药效研究及临床应用概况[J].江苏中医药,2012,43(1):69.
[5] 华峰.驱风一字散加味联合穿心莲滴眼液治疗春季结膜炎临床观察[J].基层园地,1998,8(1):56.
[6] 焦灵利.荆防抗感泡腾片的研制与药效学研究[D].南京:南京中医药大学,2007.
[7] 曾南,沈映君,刘旭光,等.荆芥挥发油抗炎作用研究[J].中药药理与临床,1998,14(6)∶24.
[8] 李淑荣,唐光菊.荆芥与防风的药理作用研究[J].中药材,1989,12(6):37.
[9] 葛卫红. 荆芥、防风挥发油抗炎作用的实验研究[J].成都中医药大学学报,2003,25(1):55.
[10] 朱慧,张良,喻斌,等. 荆芥内酯的一般药理学研究[J]. 中国实验方剂学杂志,2011,17(6):237.
[11] 钱雯,单鸣秋,丁安伟.荆芥饮片HPLC指纹图谱研究[J].中成药,2011,33(5):733.
[12] 胥庆华,刘丽云,赵瑞华.中药药对大全[M]. 北京:中国中药出版社,1996:360.
HPLC specific chromatograms of drug pair of Schizonepetae
Herba and Saposhnikoviae Radix
YU Li-xia,SHAN Ming-qiu,DING An-wei*
(Jiangsu Key Laboratory for Traditional Chinese Medicine Formulae Research,Nanjing University of
Chinese Medicine,Nanjing 210023,China)
[Abstract] In this experiment,the HPLC specific chromatogram was adopted,with Agilent Extend-C18 (4.6 mm×250 mm,5 μm) as the chromatographic column,and 0.5‰ trifluoroacetic acid and acetonitrile as the mobile phase for gradient elution,so as to establish specific chromatograms for drug pair of Schizonepetae Herba and Saposhnikoviae Radix from different producing area,identify 12 common characteristic peaks,and obtain the comparison specific chromatography of drug pair of Schizonepetae Herba and Saposhnikoviae Radix. The method is simple,accurate and highly reproducible,and thus can be used as the basis for the quality control of the drug pair.
[Key words] Schizonepeta Herba;Saposhnikovia Radix;drug pair;specific chromatogram
doi:10.4268/cjcmm20140425, 百拇医药(于丽霞 单鸣秋 丁安伟)