芸薹子化学成分研究(3)
化合物8 白色固体(丙酮),ESI-MS m/z 399.1[M+H]+?1 H-NMR(CDCl3,600 MHz)δ: 5.35(1H,t,J=2.6 Hz,H-6),5.18(2H,m,H-22,23),1.02(3H,s,H-19),1.01(3H,d,J=6.4 Hz,H-21),0.92(3H,d,J=6.8 Hz,H-28),0.83(3H,d,J=6.8 Hz,H-26),0.82(3H,d,J=6.8 Hz,H-27),0.69(3H,s,H-18); 13C-NMR(CDCl3,150 MHz)δ: 37.2(C-1),28.5(C-2),71.8(C-3),38.3(C-4),140.7(C-5) ......
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