【摘 要】 目的：建立测定斯达舒中铝含量的新方法。方法：以萘甲醛席夫碱为络合剂，采用荧光分光光度法，在醋酸铵-醋酸(pH=7)的缓冲溶液中测定斯达舒中铝的含量。结果： 在激发波长为437 nm，发射波长为525 nm处，用荧光分光光度法对浓度0～6 μmol/L范围内铝离子标准溶液进行荧光强度的测定，结果表明荧光强度和浓度具有较好的线性关系，平均加样回收率为99.02%～102.03%，准确度较好。结论：该方法选择性好、灵敏度高、响应时间短、操作简便，适合于胃药斯达舒中铝含量的测定。

    【关键词】 铝；荧光分光光度法；斯达舒

    【中图分类号】R914.1 【文献标志码】 A 【文章编号】1007-8517(2018)08-0034-03

    Abstract：Objective To establish a new method for the determination of aluminium in Si Dashu. Method The content of aluminum in Si Dashu was determined in ethanoic acid-ammonium acetate cushion fluid ( pH=7) with naphthalene formaldehyde Schiff base as complexing agent by fluorescence spectrophotometry. Result The calibration curve of aluminum ion with good linearity was obtained over the range of 0-6 μmol/L at the excitation wavelength of 437 nm and the emission wavelength of 525 nm. The recovery rate was 99.02%～102.03% with good accuracy. Conclusion The method has the advantages of high sensitivity ......