【摘 要】：目的：建立上清丸的质量控制方法。方法：采用高效液相色谱法测定方中君药黄芩中黄芩苷的含量，同时对大黄和黄柏进行薄层色谱鉴别。结果：黄芩苷进样量在0.3384～0.9024μg(r＝0.9999)与峰面积呈良好的线性关系，平均加样回收率为：98.64%，RSD为0.88%(n＝6)；薄层色谱斑点清晰，阴性对照无干扰。结论：该方法准确，重现性好，可用于上清丸的质量控制。

    【关键词】：上清丸质量标准薄层色谱法高效液相色谱法黄芩苷

    【中图分类号】R914.1；R944.2+2【文献标识码】A【文章编号】1007-8517(2008)08-0035-03

    Quality Standards Research of Shangqing Pills

    Xiao yan

    Huaihua Institute for Drug Control，Hunan Huaihua，China 418000

    Abstract Objective To establish the method for quality control of Shangqing Pills. MethodsThe Baicalin in Radix Scutellariae was determined byHPLC ......